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This data release presents the concentration of zinc, oxygen, pH, temperature, and the time point at which measurements were taken for experimental oxidation work regarding zinc and copper sulfide minerals. These data accompany the following publication: Gartman, A., Whisman, S.P., and Hein, J.R., 2020, Interactive oxidation of sphalerite and covellite in seawater: implications for seafloor massive sulfide deposits and mine waste: ACS Earth and Space Chemistry, https://doi.org/10.1021/acsearthspacechem.0c00177, where they are also presented as Supplemental Table 1.