Filters: Tags: Gas Chromatography (X)
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Polycyclic aromatic hydrocarbons (PAHs) are reported for water samples collected from the San Lorenzo River water during the rainy seasons from 2015 to 2016. Samples were collected during 2-, 5- and close to 10 year flood events.
This data release comprises a set of environmental sucralose occurrence data in the Sacramento area. Groundwater samples were collected throughout the Sacramento Valley as part of the California Groundwater Ambient Monitoring and Assessment Program Priority Basin Project study in the Sacramento area. These water samples were analyzed for sucralose by chemical derivatization followed by gas chromatography mass spectrometry. The calculated concentrations of sucralose detected in the water samples and the associated quality assurance data are tabulated in this data release. This data release supports the following publications: [Voss et al, in prep]
Categories: Data;
Tags: California,
Sacramento,
USGS Science Data Catalog (SDC),
United States,
Water Quality,
Analysis of biological tissues or direct sources of food may better characterize exposure of non-target organisms to current-use pesticides. Food boluses were collected from tree swallow (Tachycineta bicolor) nestlings using a non-lethal, ligature method and were composited based on nest. The ligatures, which prevented the bolus from being swallowed, were placed on nestlings for 1 h until samples were collected. Samples in 2016 were collected from nestlings at 6 days and 12 days post-hatch whereas 2018 samples were collected from nestlings at 12 days post-hatch. Furthermore, in 2016 and 2018, insects commonly consumed by tree swallows were collected via sweep net and composited based on suborder (Brachycera, Nematocera,...
This dataset contains measurements of dissolved hydrocarbons in from groundwater samples collected in the shale gas producing regions of West Virginia, USA, between June and August of 2018. The target analytes in this study were: methane (CH4), ethane (C2H6), ethene (C2H4), ethyne (C2H2), propane (C3H8), propene (C3H6), i-butane (C4H10), n-butane (C4H10), 1-butene (C4H8), propyne (C3H4), i-pentane (C5H12), n-pentane (C5H12), 2-methyl-pentane (C6H14), 3-methyl-pentane (C6H14), hexane (C6H14), and benzene (C6H6). This dataset also contains corresponding measurements of chlorofluorocarbons (CFCs), Sulfurhexafluoride (SF6), dissolved permanent gases (N2/Ar), tritium, the isotope ratio of helium dissolved in water, the...
Categories: Data;
Tags: Energy Resources,
Environmental Health,
Geochemistry,
USGS Science Data Catalog (SDC),
USGS-EMA-LOW-SS Oil and gas,
This dataset contains measurements of dissolved hydrocarbons in various water sources, as well as ancillary raw calibration data showing the stability of the gas chromatograph with an atomic emission detector and flame ionization detector (GC-AED-FID) analytical system over time. Across multiple studies, samples from tap water, groundwater, surface water, springs, mine outflows, and blank materials were analyzed using this system over a period from 2014 to 2017, comprising 172 samples analyzed. In addition to water samples, 183 calibrations conducted over the same period of time are included to document the stability of the GC-AED-FID system over time. The target analytes in this study were: methane (CH4), ethane...
Categories: Data;
Tags: AED,
Atomic Emission Detector,
Energy Resources,
FID,
Flame Ionization Detector,
Results of lipid biomarker concentration and compound specific isotopes analyzed from authigenic carbonates and surrounding sediment collected from Baltimore and Norfolk seep fields along the United States Atlantic Margin are presented in csv format. Samples were collected by the U.S. Geological Survey and Duke University between 2012 and 2015 using remotely operated vehicles (ROVs). Geochemical analysis was performed using gas chromatography (GC) and GC-combustion isotope ratio mass spectrometry (GC-C-IRMS).
Soil gas methane and combustible gas concentrations collected from oil and gas well pad locations in Utah. Soil gas samples were measured on site and/or collected for later analysis as described in supporting documentation. Multiple sample locations around well head and depths within the soil profile are available for select sites. Supporting documents provide information of sample collection protocol and data quality assurance.
Categories: Data;
Types: Map Service,
OGC WFS Layer,
OGC WMS Layer,
OGC WMS Service;
Tags: Big Flat,
Big Indian North,
Big Indian South,
Big Valley,
Bluebell,
A multiresidue method for solids (i.e., soil, sediment, sludge) was developed and evaluated for the analysis of pesticides and pesticide degradates. Initially, a well characterized soil was used to determine the recovery of target compounds using an Energized Dispersive Guided Extraction (EDGE) system with two extraction solvents, acetonitrile and 1:1 (v/v) hexane:acetone. Extracts were cleaned using solid-phase extraction (SPE) with graphitized carbon cartridges and three elution solvents, acetonitrile, dichloromethane, and 1:1 (v/v) dichlormethane:ethyl acetate. The individual SPE elutions from the two extraction solvents were analyzed separately via GC-MS/MS and LC-MS/MS for 210 pesticides and pesticide transformation...
Categories: Data;
Tags: Environmental Health,
USGS Science Data Catalog (SDC),
biosolids,
contaminant transport,
environment,
Acetylene (C2H2) is a molecule rarely found in nature, with few known natural sources, but acetylenotrophic microorganisms can use acetylene as their primary carbon and energy source. As of 2018 there were 15 known strains of aerobic and anaerobic acetylenotrophs, however we hypothesized that there may be yet unrecognized diversity of acetylenotrophs in nature. In this study, we expanded this diversity by isolating an aerobic acetylenotroph, Bradyrhizobium sp. strain I71, from trichloroethene (TCE)-contaminated soils undergoing bioremediation. TCE-contaminated soils from the NASA Ames Research Center in California were used to establish soil microcosms with acetylene as the primary carbon substrate and acetylene...
This data release presents the results of analyses of biota and water samples collected on multiple dates from 2007 to 2014 at 3 locations in Lake Mead National Recreation Area. Data are presented in 3 spreadsheets containing sample analyses for (1) stable isotopes in biota (2007-2014), (2) synthetic organic compounds in biota (2013-2014), and (3) synthetic organic compounds in water (2013-2014)
Oil and gas (OG) wastewaters are commonly disposed of by underground injection and previous research showed that activities at a disposal facility in West Virginia affected stream biogeochemistry and sediment microbial communities downstream from the facility. Microorganisms can control the fate and transport of organic and inorganic components of OG wastewater highlighting the need to characterize the effects of OG wastewater components on microbial activity. We conducted a series of aerobic microcosm experiments to assess the influence of high total dissolved solids (TDS) and hydraulic fracturing fluid additives (2,2-dibromo-3-nitrilopropionamide (DBNPA), a biocide, and ethylene glycol, an anti-scaling additive),...
Categories: Data;
Tags: Biochemistry,
DNA sequencing,
Energy Resources,
Environmental Health,
Fayette County,
Data Release for "Comparability and reproducibility of biomarker ratio values measured by GC-QQQ-MS"
This data release includes biomarker ratio values calculated from measurements made at the USGS for the reference oil NSO-1 that were reported in a journal article entitled Comparability and reproducibility of biomarker ratio values measured by GC-QQQ-MS (French et al., 2020).
Categories: Data;
Tags: Energy Resources,
NSO-1,
USGS Science Data Catalog (SDC),
gas chromatography,
geoscientificInformation,
Time-series of sediment chemistry, including organic biomarker composition and bulk inorganic geochemical analytes, from samples collected over a one-year period in a sediment trap. The sediment traps were deployed at a depth between 603 m to 1318 m, and they were programmed to rotate a 250 mL sample bottle at 30 d intervals, delivering 12 samples during the 1-year deployment between August 2012 and June 2013. In addition, dissolved water column nutrient concentrations and water column trace element particulate concentrations were collected in Baltimore Canyon on the U.S. Mid-Atlantic Bight (MAB).
Categories: Data;
Types: Citation;
Tags: Assessments,
Atlantic Ocean,
Atlantic Ocean,
Baltimore Canyon,
animal-sediment interactions,
This dataset was produced from analyzing Affinisep SDB-RPS, Affinisep HLB, and Restek Resprep C18 disks that were deployed with the use of Chemcatcher® passive sampling devices. Silicone bands were also deployed and used for exploring economical methods of sampling for pesticides in surface water. Sampling assemblies were deployed in streams throughout the foothills of the Sierra Nevada range and California's northern Central Valley from 2017 to 2019. Samples were extracted in situ then eluted and concentrated at the Organic Chemistry Research Laboratory in Sacramento, CA. Samples from silicone bands were extracted via agitation in appropriate solvents. Samples were analyzed for a suite of 155 pesticides and degradates...
This U.S. Geological Survey (USGS) Data Release is focused on the geochemistry of wells within the oil zone and groundwater monitoring wells away from the oiled zone at the National Crude Oil Spill Fate and Natural Attenuation Research Site, Bemidji MN (USA) from 1985-2015. The site located in Beltrami County is where a high-pressure pipeline carrying crude oil burst in 1979 and spilled approximately 1.7 million liters (10,700 barrels) of crude oil into glacial outwash deposits. Researchers and scientists from government agencies, academic institutions, the regulatory community, and private companies have conducted extensive investigations of groundwater geochemistry in hopes of understanding the evolution of plumes...
The data release contains biomarker data generated by Gas Chromatography-Single Quadrupole Mass Spectrometry in the Petroleum Geochemistry Research Laboratory. The data was used to determine the precision and accuracy of one daily operating standard for the method entitled, "Petroleum Geochemistry Research Laboratory Method for Qualitative Biomarker Analysis of Crude Oil and Rock Extracts by Gas Chromatography-Single Quadrupole Mass Spectrometry".
Categories: Data;
Tags: Energy Resources,
USGS Science Data Catalog (SDC),
biomarkers,
gas chromatography,
geoscientificInformation,
The Marcellus Shale Energy and Environmental Laboratory (MSEEL) field site in Morgantown, WV was established by West Virginia University in order to increase understanding of factors that affect resource recovery and environmental impacts from unconventional oil and gas development. The site, which is located in the Morgantown Industrial Park (MIP) adjacent to the Monongahela River, includes one well pad which hosts four horizontal gas wells that target the Marcellus Shale approximately 7400 ft below ground level. As part of the MSEEL study, the MIP 5H well was drilled in 2015. Water samples were collected from the holding pond used to hydraulically fracture the MIP 5H well (API 47-061-01699), and a time series...
Categories: Data;
Tags: City of Morgantown,
Energy Resources,
Environmental Health,
Geochemistry,
Hydrology,
This dataset presents the results of analysis of aquatic biota tissue samples, collected over multiple sampling events from in from 2007 to 2014 at three sites (Las Vegas Bay, Overton Arm, and Boulder Basin) in Lake Mead National Recreational Area. The tissue samples were analyzed for concentrations of Carbon 13 and Nitrogen 15 isotopes by the University of California, Davis in Davis, California. Data are presented in 1 spreadsheet worksheet that is organized by year, location, and taxa. General trophic level (Vander Zanden and Rasmussen, 1999) and calculations of benthic reliance (Umek and others, 2010) also are included. Combined data from sampling events in 2007 and 2008 previously were published in Umek and...
Categories: Data;
Tags: Boulder Basin,
Colorado River,
Lake Mead,
Lake Mead National Recreational Area,
Las Vegas,
This dataset presents the results of passive water sampling conducted at 2 sites in 2013 and 3 sites in 2014 in Lake Mead National Recreational Area. Polar Organic Chemical Integrative Samplers (POCIS) and Semipermeable Membrane Devices (SPMDs) were deployed in Las Vegas Bay and Overton Arm in 2013 and Las Vegas Bay, Boulder Basin, and Overton Arm in 2014. The samplers were analyzed for concentrations of polychlorinated biphenyls (PCBs), organochlorines (DDT-type compounds and their degradates), polybrominated biphenyl ethers (PBDEs), polycyclic aromatic hydrocarbons (PAHs), waste indicators (WW), and yeast estrogen screen (YES) by the U.S. Geological Survey (USGS) at the Columbia Environmental Research Center (CERC)...
Categories: Data;
Tags: Boulder Basin,
Colorado River,
Lake Mead,
Lake Mead National Recreational Area,
Las Vegas,
To better understand the potential pesticide exposure, samples were collected from locations along two creeks in Pinnacles National Park and four creeks in nearby Bureau of Land Management (BLM) lands. Silicone bands were used as passive sampling devices (PSD) staked in the creek and above in the air (above the water line). Sampling was conducted in the summer from 2019 to 2021. PSDs were deployed for 2 to 4 weeks and sediment was collected once in 2020. PSDs were extracted via sonication with an organic solvent and sediment was extracted via pressurized liquid extraction and solid phase extraction cleanup. Samples were analyzed for 168 pesticides and degradates using both gas and liquid chromatography-tandem mass...
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