Filters: partyWithName: Geology, Energy & Minerals Science Center (X) > partyWithName: U.S. Geological Survey (X) > partyWithName: Eric A Morrissey (X)
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To test if reflectance increases to sedimentary organic matter (vitrinite) caused by broad ion beam (BIB) milling were related to molecular aromatization and condensation, we used Raman and Fourier transform infrared (FTIR) spectroscopies to evaluate potential compositional changes in the same vitrinite locations pre- and post-BIB milling. The same locations also were examined by atomic force microscopy (AFM) to determine topographic changes caused by BIB milling (as expressed by the areal root-mean-square roughness parameter Rq). Samples consisted of four medium volatile bituminous coals. We used a non-aggressive BIB milling approach with conditions of [(5 min, 4 keV, 15°incline, 360° rotation at 25 rpm and 100%...
Categories: Data;
Tags: Bituminous Coal,
Broad Ion Beam,
Coal resources,
Energy Resources,
Geochemistry,
At recent technical conferences, many coal geoscientists in academia and government institutions as well as in industry organizations have expressed concern about the dwindling number of students and young staff members interested in careers in coal geoscience. To better understand what is driving these trends and to identify potential ways that the community can increase interest and participation in coal geoscience, two different surveys were sent to 94 coal geoscientists who were current or past members of The Society of Organic Petrology (TSOP) in February 2020. As the trends and perceptions in industry and government organizations may be different than in universities, one distinct survey was sent to members...
Inorganic compositions of flowback and co-produced waters from hydrocarbon extraction have been studied directly and through laboratory experiments that seek to replicate subsurface water-rock interaction. Here a broad analysis is made of compositions from the U.S. Geological Survey Produced Waters Database (v2.3) and leachates (water, hydrochloric acid, artificial brine) for 12 energy-resource related shales from across the United States. The database illustrates common ranges for 26 elements in 4 produced water types and enhanced solubility with increasing ionic strength is observed for Al, Ba, Fe, Li, Mn, Rb, Sr, and possibly 11 other elements. Differences are observed between laboratory leachates and produced...
These data represent laboratory reflectance measurements conducted on a suite of sandstone, tuffaceous mudstone and claystone rocks and sediment, which are known host and source materials for roll front Uranium deposits mined throughout the South Texas Coastal Plains. Visible through Near Infrared through Shortwave Infrared (~0.4 - 2.5 microns) reflectance were measured using an artificial light source attached to an Analytical Spectral Devices (ASD) spectrometer. A total of 125 spectra were measured and analyzed, representing samples from nine former open-pit mine sites excavating rocks from four different mapped geologic units, including rocks and sediments from the Jackson Group, Catahoula, Oakville and Goliad...
This study describes the application of organic petrology techniques to quantify the amount of coal and carbonaceous combustion by-products (i.e., coke, coal tar/pitch, cenospheres) in sediments taken from the Kinnickinnic River adjacent to the former site of the Milwaukee Solvay Coke and Gas Company. The site produced metallurgical coke and coal-gasification by-products from 1902-1983 and was assessed in 2001 as a potential Superfund site in part due to high levels of polycyclic aromatic hydrocarbons (PAHs) which readily absorb to coal and combustion by-products.
Note: this data release is currently being revised and is temporarily unavailable. This dataset covers Rock-Eval and reflectance data.
The nanoscale molecular composition of kerogen is a challenging parameter to characterize given the chemical and structural complexity exhibited by this important biopolymer. However, kerogen composition will strongly impact its reactivity and so is a critical parameter to understand petroleum generation processes during kerogen catagenesis. The recent advent of tip-enhanced analytical methods, such as atomic force microscopy-based infrared spectroscopy (AFM-IR), has allowed for the major compositional features of kerogen to be elucidated at spatial resolutions at or below 50 nm. Here we apply AFM-IR to examine inertinite, an important kerogen maceral type, from an immature Eagle Ford Shale sample. Our data show...
Categories: Data;
Tags: Atomic force microscopy-based infrared spectroscopy (AFM-IR),
Energy Resources,
Geochemistry,
Organic matter,
Shale,
Solid bitumen is a petrographically-defined secondary organic matter residue produced during petroleum generation and subsequent oil transformation. The presence of solid bitumen impacts many shale reservoir properties including porosity, permeability, and hydrocarbon generation and storage, amongst others. Furthermore, solid bitumen reflectance is an important parameter for assessing the thermal maturity of formations with little to no vitrinite. While the molecular composition of solid bitumen will strongly impact associated parameters such as the development of organic matter porosity, hydrocarbon generation, and optical reflectance, assessing the molecular composition of solid bitumen in situ within shale reservoirs...
Categories: Data;
Tags: Energy Resources,
Geochemistry,
Oil and gas resources,
Organic matter,
Shale,
As more hydrocarbon production from hydraulic fracturing and other methods produce large volumes of water, innovative methods must be explored for treatment and reuse of these waters. However, understanding the general water chemistry of these fluids is essential to providing the best treatment options optimized for each producing area. Machine learning algorithms can often be applied to datasets to solve complex problems. In this study, we used the U.S. Geological Survey’s National Produced Waters Geochemical Database (USGS PWGD) in an exploratory exercise to determine if systematic variations exist between produced waters and geologic environment that could be used to accurately classify a water sample to a given...
Waters co-produced during petroleum extraction are the largest waste stream from oil and gas development. Reuse or disposal of these waters is difficult due both to their high salinities, which can greatly exceed 35 g/L (seawater equivalent), and also the sheer volume of wastewater generated, which is estimated at nearly 900 billion gallons per year across the United States. Beyond disposal concerns, produced water may also represent a possible source of valuable mineral commodities. While an understanding of the trace element composition of produced water is required for evaluating the associated resource and waste potential of these materials, measuring trace elements in high salinity brines is challenging due...
Subsurface microbial (biogenic) methane production is an important part of the global carbon cycle and has resulted in natural gas accumulations in many coal beds worldwide. Laboratory experiments indicate coal beds can act as natural geobioreactors and produce additional low carbon renewable natural gas with algal or yeast compounds, yet the effectiveness of these nutrients in situ are unknown. This study uses down-well monitoring methods in combination with deuterated water (99.99% D2O) and a 200-liter injection of 0.1% yeast extract to stimulate and isotopically label newly generated methane. A total dissolved gas pressure sensor was placed down-well into the Flowers-Goodale coal bed at the USGS Birney Test Site...
The USGS Gulf Coast Source Rock Database (GCSRD) is an online repository for all publicly available source rock data (outcrop and subsurface) from the states of Florida, Georgia, Alabama, Mississippi, Louisiana, Arkansas, and Texas. "Source rock data" are defined in this context as data that include any of the following measured or calculated parameters: -total organic carbon (TOC), -various pyrolysis measurements (Tmax, S1, S2, S3, HI, OI), -vitrinite or bitumen reflectance values. All data in the GCSRD have been extracted from previously published peer-reviewed literature or as USGS-released data sets; no new measurements are included. The underlying data set is presented as an interactive, map-view application...
Categories: Data,
Data Release - Revised;
Tags: Alabama,
Louisiana,
Mississippi,
Texas,
USGS Science Data Catalog (SDC),
Numerical modeling was performed to analyze the impacts of potential multiphase conditions on long-term subsurface pressure evolution in subsurface systems. An example site on the Bruce Peninsula in Southern Ontario, Canada was selected due to the large amount of available, high-quality data showing significantly underpressured water and the possible presence of gas phase methane. The system was represented by a 1-D model in which multiphase flow and hydromechanical coupling during the last glacial loading and unloading cycle were simulated. Single-phase flow simulations were performed with the USGS single-phase flow simulator SUTRA, and then both single- and multiphase simulations were performed with the multiphase...
Types: Map Service,
OGC WFS Layer,
OGC WMS Layer,
OGC WMS Service;
Tags: Canada,
Energy Resources,
Great Lakes,
Groundwater,
Groundwater Model,
This data release contains programmed pyrolysis, organic petrographic (reflectance), and semiquantitative X-ray diffraction mineralogy data for subsurface coal and shale samples from around the world. Samples were subjected to hydrous or anhydrous pyrolysis experiments at varying temperatures and the resulting residues were analyzed via programmed pyrolysis and reflectance to document changes in thermal maturity.
The United States Gulf Coast Basin Curated Wells and Logs Database (CWLDB) is an online repository with stratigraphic information for petroleum wells in the United States portion of the onshore Gulf of Mexico Basin that provides several of the following attributes: a) deep penetrations (generally, total depth of 10,000 feet or more), b) high quality and diverse geophysical well log suites, c) lithostratigraphic logs, d) biostratigraphic units (biozones) and reports, and/or e) core or cuttings samples. First release: March 2023 Revised: November 2023 (ver. 2.0)
Citation Note: These data were collected as part of a research study published in Marine and Petroleum Geology. Please reference the following paper when citing these data: Botterell, P.J., Houseknecht, D.W., Lillis, P.G, Barbanti, S.M., Dahl, J.E, and Moldowan, J.M., 2021. Geochemical advances in Arctic Alaska oil typing – North Slope oil correlation and charge history. Marine and Petroleum Geology 127, https://doi.org/10.1016/j.marpetgeo.2020.104878. The Arctic Alaska petroleum province is geologically and geochemically complex. Mixed hydrocarbon charge from multiple source rocks and/or levels of thermal maturity is common within an individual oil pool. Biomarker and chemometric statistical analyses were used...
Categories: Data;
Tags: Alaska,
Arctic National Wildlife Refuge,
Biomarkers,
Energy Resources,
North Slope,
We developed a methodology to estimate maximum brine injection rates in subsurface formations across wide geographic areas using inverse modeling-based optimization techniques. We first defined geographic areas where groundwater was too saline to meet the standard for drinking water and where sufficient confining units existed above and below the injection layers. We then assumed concurrent brine injection into a system of wells on a consistent 25 km x 25 km spacing across the entire modeled area. Taking advantage of symmetry, we represented each 25 km x 25 km injection area as a 12.5 km-long one-dimensional radial model, divided into 100 logarithmically-sized grid blocks. A single layer of grid blocks was used...
Citation Note: These data were collected as part of a research study published in Environmental Science and Technology. Please reference the following paper when citing these data. Blondes, M.S., Shelton, J.L., Engle, M.A., Trembly, J.P., Doolan, C.A., Jubb, A.M., Chenault, J.M., Rowan, E.L., Haefner, R.J., and Mailot, B.E., 2020, Utica Shale Play Oil and Gas Brines: Geochemistry and Factors Influencing Wastewater Management: Environmental Science & Technology, https://dx.doi.org/10.1021/acs.est.0c02461. The Utica and Marcellus Shale Plays in the Appalachian Basin are the 4th and 1st largest natural gas producing plays in the United States. Hydrocarbon production generates large volumes of brine (“produced water”)...
Categories: Data;
Tags: Appalachian Basin,
Energy Resources,
USGS Science Data Catalog (SDC),
field sampling,
natural gas resources,
To better understand the possible risks posed to shallow groundwater resources by geologic carbon sequestration (GCS), a multi-scale numerical modeling approach was invoked using the TOUGHREACT code from Lawrence Berkeley National Laboratory. The code solves coupled equations representing conservation of mass and energy on a finite difference grid to simulate multiphase, multicomponent, non-isothermal heat and mass transport in porous media. Two different two-dimensional cross-section modeling domains were constructed to improve understanding of groundwater flow and contaminant transport processes at a field site in soutwestern Utah. The site represents a natural analogue for leakage from a GCS site because water...
Researchers at the U.S. Geological Survey (USGS) and their collaborators conducted a study of the geochemical properties of coals currently produced for electric power generation in the Illinois Basin in Illinois and Indiana. The study follows from recommendations by an expert panel for the USGS to investigate the distribution and controls of trace constituents such as mercury (Hg) in Illinois Basin coals and the behavior of these constituents in coal preparation. A total of 72 new samples were collected by USGS collaborators. These samples include raw coals, prepared coals, and waste coals from coal preparation. To understand the geochemistry and cleaning behavior of these coals, these samples were subjected to...
Categories: Data,
Data Release - Revised;
Tags: Coal,
Daviess County,
Dubois County,
Elemental analysis,
Energy Resources,
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